Plastic Analysis
Manufacturer & Model | |
DEA 288 Ionic, NETZSCH-Gerätebau | |
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Monitors temperature-dependent changes in polymers via dielectric properties | |
Key Features | |
Heating rate | 0.001 to 10 K/min |
Temperature range | 20 to 250 °C |
Frequency range | 1 mHz to 1 MHz |
UV curing | OmniCure S2000 |
Technical descriptionDielectric Analysis (DEA) uses the dielectric properties of polymers. For this purpose, the professorship is equipped with the DEA 288 Ionic from NETZSCH. By applying a sinusoidal voltage, the response of the polymer is measured via two electrodes. In this way, the melting and crystallization of semi-crystalline thermoplastics can be determined. The curing of thermosets can also be measured using a connectable UV lamp. The great advantage of DEA is the immense measuring frequency spectrum from 1 mHz to 1 MHz with which the plastic can be measured. Current research at the professorship is concerned with quantifying the measurement signal for thermoplastics and using it as an in-situ measurement technique in the PBF-LB/P process. |
Manufacturer & Model | |
DSC 300 Caliris Select, NETZSCH-Gerätebau | |
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Detects temperature-dependent phase transitions and physical changes | |
Key Features | |
Heating rate | 0.001 to 500 K/min |
Temperature range | -40 to 600 °C |
Mechanical press | Cold-sealing of crucibles |
Software | Proteus 9 |
Technical descriptionThe NETZSCH DSC Caliris 300 Differential Scanning Calorimetry (DSC) instrument is used for the thermal analysis of plastics. The DSC can be used to determine essential polymer properties such as glass transition ranges, melting and crystallization ranges, and specific heat capacities. Knowledge of these values is important for later use in the additive manufacturing process. For example, DSC can be used to detect powder aging. In addition to determining temperature peaks and enthalpies, the “Proteus" evaluation software allows an unknown material to be automatically identified by database comparison. |
Manufacturer & Model | |
Mastersizer 2000, Malvern Panalytical | |
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Measuring particle size distribution | |
Wet and dry dispersion for various sample types | |
Key Features | |
Particle size range | Particles from 0.1 µm to 3500 µm |
Measurement technique | Laser diffraction |
Sample preparation | Accommodates dry powders and suspensions |
Throughput | Rapid analysis with results in under 30 seconds |
Technical descriptionThe Mastersizer 2000 by Malvern Panalytical is a laser diffraction particle size analyzer. It measures the size distribution of particles in a sample by analyzing how a laser beam is scattered as it passes through the sample. The system is used across various industries, including additive manufacturing and materials science, to ensure consistent quality and performance of products by providing precise and reproducible particle size data. |
Manufacturer & Model | |
Mflow, Zwick Roell | |
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Testing according to DIN EIN ISO 1133 | |
Displacement sensor for continuous melt volume rate measurement | |
Key Features | |
Weights | 0.325 kg, 2.16 kg, and 5 kg |
Temperature range | up to 400 °C |
Technical descriptionMelt flow indexing is a critical method for evaluating the quality and consistency of polymer powders used in laser sintering processes. In our research, we utilize melt flow indexing to monitor and ensure the uniformity of powder characteristics before processing. This technique involves measuring the melt mass volume rate (MVR), which reflects the material's viscosity and flow behavior when subjected to heat. By analyzing these properties, we can detect changes in powder quality and predict how aging due to high processing temperatures might affect the material. This method aligns with the DIN EN ISO 1133 test standard and helps maintain optimal powder performance by confirming that the MVR falls within a predefined range, ensuring reliability and precision in our additive manufacturing processes. |